Advanced
Course on "Photoelectron Spectroscopy Using X-rays"
(Feb- May 2005)
Last Class on : 4May in Lecture Hall at 9:30 am
25
Registerd and 15 Unregistered Participants are attending the course.
13
Participants are from Utkal University Physics Department.
2
Participants are from Institute of Material Science.
XPS Laboratory Schedule:
First Lab Visit : 28Feb & 2March (System demonstration) Group/Timing
Second LabVisits : 20 Apr & 25 Apr (ARXPS experiments on SiO2/Si and GeO/Ge) Groups/Timings
Third
LabVisits : 27 Apr & 2 May
(Data
Analysis)
Groups/Timings
Topics Covered in the course :
(1) 2nd
Feb
Introduction to XPS and AES
(2)
7th
Feb
Basic Principles and technique of XPS and AES
(3)
9th
Feb
Vacuum Techniques, Ion Neutralisation Spectroscopy.
(4) 28th
Feb
Laboratory : Introduction to XPS system at IOP
(5)
2nd
Mar
Laboratory : Introduction to XPS system at IOP
(6)
7th
Mar
Photon sources : Theory and Working
(7)
9th
Mar
Mg, Al sources,Monochromator, Dipole selection Rules,
Electron Microprobe Analysis
(8)
14th Mar
Anlysers, RFA, CMA
(9)
21st
Mar
Parallel Plate analyser, CMA
(10)
24th Mar
CHA, Analysers in AES &XPS, channeltron
(11) 4th
April
Spectral Interpretation, nomenclature
(12)
6th April
Spectral interpretations in AES
(13)
11th April XPS
spectral interpretatons, chemical shifts
(14)
13th April Valence
band studies, Intensity variations with depth &
angle, ARXPS
(15)
18th April
Quantification with XPS and AES
(16)
20th April
Laboratory : XPS experiments on SiO2/Si
(17) 25th
April
Laboratory : XPS experiments on GeO/Ge
(18)
27th April
SiO2/Si spectra, smootheing, background removal,
Curve fitting, concentration of elments.
(19) 2nd
May
Analysing GeO/Ge spectra.
(20)
4th
May
Using XPS intensity for overlayer thickness, conc.,
modes of growth evaluation, line shape, ARXPD.
Main Books :
Practical
Surface Analysis by Auger and X-Ray Photoelectron
Spectroscopy
: Briggs and M.P. Seah
An
Introduction to X-Ray Spectroscopy :
B.K. Agarwal (Springer Series in Optical Sciences, vol.15)
Electron
Spectroscopy: Theory, Techniques and Application:
edited By C.R. Brundle and A.D. Baker
(Academic Press.)
Building Scientific
Apparatus: A practical guide to Design and Construction:
by J.H. Moore,
C.C. Davis, M.A. Coplan
Photoelectron
Spectroscopy : Stefan Hufner
(Springer Series in Solid State Sciences, vol.82)
Core
Level Spectroscopy in Condensed Syatems:
edited by J. Kanamori and A. Kotani
(Springer Series in Solid State Sciences, vol.81)
X-ray
Spectroscopy: edited by L. V.
Azaroff (McGraw Hill Book Company)
Modern Techniques of
Surface Science: D.P. Woodruff and
T.A. Delchar (Cambridge Solid State Science Series)
Electronic Properties of
Surfaces : M. Prutton
Practcal
Guide to Surface Science and Spectroscopy : Y.W.
Chung (Academic Press)
Experimental
Innovations in Surface Science -A Guide to Practical Laboratory
Methods and Instruments:
John T. Yates, Jr. (AIP Press)
Solid
state Physics : N.W. Ashcroft and
N.D. Mermin
Physics
at Surfaces: A. Zangwill (Cambridge
University Press)